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DIY Phosphate Reactor

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jfinch View Drop Down
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    Posted: October 04 2006 at 11:41pm

The DIY forum is my favorite forum here and it has really been dying off the last few months so I'm hoping to do my part in reviving it Big%20smile.  I had a few hours to kill last night and I've been battling cyano lately so I decided to build a fluidized phosphate reactor.  Hope someone else finds this helpful or interesting...

This was kind of a spur of the moment project so most of the stuff I just had on hand, but ymmv.  The main reaction chamber is an 11" length of 3" acrylic tubing.  I was lazy so I made the flanges square rather then round.  Here's the build pictures.
 
The bottom, 1/8" white acrylic (it's what I had laying around), being glued to the tube.
 
 
This is the flange top setup.  I used double sided tape to stick two 1/4" thick flange pieces together and then drilled through both pieces for the flange bolts using a 3/16" bit.  I then used a 2 1/2 inch hole saw to drill a hole in the center of only one flange (the one glued to the tube).
 
 
I'm now using a 1/4" tap to add threads to the bottom flange:
 
 
I always use the "pins" method when gluing acrylic.  You can see three straight pins keeping the tube lifted off the flange.  A needle bottle is used to wick Weld-on 4 cement into the space between the tube and flange.  I let it sit like this for about 2 minutes before removing the pins and letting the pieces "melt" together.
 
 
I was pretty sloppy from trying to take the above picture but as you can see it's a pretty good bubble free joint.
 
 
For the top flange I drilled a 7/8" hole in the center to fit the inlet piping.  I also drilled a 5/8" hole for the outlet piping.  This picture shows the 5/8" hole being tapped for a 3/8" John Guest fitting.
 
 
 
The center hole will not be tapped, I'll just use a 1/2" plastic nipple, an o-ring and a couple fittings as a bulkhead fitting.  This picture shows the general layout of these fittings.  I'm using cpvc fittings and pipe because it's smaller then regular pvc.
 
 
The flange top goes between these two sections and looks like this when tightened.  The o-ring ensures a leak free seal.
 
 
The 3/16" holes in the top flange are enlarged to 5/16" for clearance of the 1/4" nylon flange bolts.  The John Guest fitting is then screwed into place.  A rubber gasket for some toilet fitting found in Lowes is used as a gasket between the flanges.  Here's an upper view before adding the flange bolts.
 
 
Here is a side view of the mostly finished product.  The water is feed into the center pipe which fluidizes the media in the reactor and finally it exits out the 3/8" fitting.
 
 
And finally, here it filled with media.  I'm using activated alumina, but iron oxide hydroxide would be a better choice.  I will likely use this reactor for activated carbon too.
 
 
How well does it work?  Awesome.  Here's a short video of me rinsing the media with tapwater showing how a fluidized reactor should look (notice the beads slowly moving up and down in the reactor).  www.xmission.com/~jfinch/music/fuidized.mov
 
 


Edited by jfinch - October 04 2006 at 11:43pm
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Gahlenfr View Drop Down
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Post Options Post Options   Thanks (0) Thanks(0)   Quote Gahlenfr Quote  Post ReplyReply Direct Link To This Post Posted: October 04 2006 at 11:56pm
Awesome job JonThumbs%20Up  I need to build one of those for activated carbon.  How did you cut the circle for the flange lid? EDIT  Sorry, I needed to look more closely at the pictureEmbarrassed  Large hole saw would do the trick and give a clean cut!

Edited by Gahlenfr - October 05 2006 at 12:09am
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Post Options Post Options   Thanks (0) Thanks(0)   Quote tileman Quote  Post ReplyReply Direct Link To This Post Posted: October 05 2006 at 12:02am
Hey Jon,  Let me know when a house in your neighborhood goes up for sale...
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Post Options Post Options   Thanks (0) Thanks(0)   Quote Mike Savage Quote  Post ReplyReply Direct Link To This Post Posted: October 05 2006 at 12:19am
That was excellent Thumbs%20Up
 
Thanks Jon.


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Post Options Post Options   Thanks (0) Thanks(0)   Quote jfinch Quote  Post ReplyReply Direct Link To This Post Posted: October 05 2006 at 8:49am
Thanks guys.
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Post Options Post Options   Thanks (0) Thanks(0)   Quote Tyrosinase Quote  Post ReplyReply Direct Link To This Post Posted: October 05 2006 at 11:57am
Is there a reason, other than aesthetics, as to why we should shoot to get bubble free joints?
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Post Options Post Options   Thanks (0) Thanks(0)   Quote jfinch Quote  Post ReplyReply Direct Link To This Post Posted: October 05 2006 at 12:22pm

Not only does it look better, but I think a bubble free joint is a stronger joint too.

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Post Options Post Options   Thanks (0) Thanks(0)   Quote fj40fax Quote  Post ReplyReply Direct Link To This Post Posted: October 05 2006 at 12:57pm
What are you using to run the water through, any powerhead I can think of would be way too much for AC?

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Post Options Post Options   Thanks (0) Thanks(0)   Quote fj40fax Quote  Post ReplyReply Direct Link To This Post Posted: October 05 2006 at 1:10pm
Another question.  Why use the wing nuts if you have threads in the bottom flange?  Can't you just use the thumb screws from the top?

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Post Options Post Options   Thanks (0) Thanks(0)   Quote jfinch Quote  Post ReplyReply Direct Link To This Post Posted: October 05 2006 at 1:11pm
I'm using my "utility" pump, an Iwaki 40.  This pump supplies water for my calcium reactor and phosphate reactor but most of it goes into the skimmer.  A valve somewhere on the inlet allows you to reduce the flow.  I haven't tried AC yet, but I think it'll work ok (I didn't add any AC in with the alumina because I'm pretty sure the AC would have floated out at the velocity needed to fluidized the alumina).

Edited by jfinch - October 05 2006 at 1:17pm
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Post Options Post Options   Thanks (0) Thanks(0)   Quote jfinch Quote  Post ReplyReply Direct Link To This Post Posted: October 05 2006 at 1:16pm
Why use the wing nuts if you have threads in the bottom flange?  Can't you just use the thumb screws from the top?

Yes I could just screw the thumbscrews down from the top.  That's what I did with my calcium reactor.  I've found that nylon screws tend to be tight in acrylic so short screws are the way to go.  But the nylon thumbscrews I had were too long and I was too lazy to cut them (I know... that's pretty lazy isn't it).  So I just screwed 'em in from the bottom and used wingnuts on the top. 
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Post Options Post Options   Thanks (0) Thanks(0)   Quote fj40fax Quote  Post ReplyReply Direct Link To This Post Posted: October 05 2006 at 1:33pm
I had a bag of carbon attached to the drain from the display on my 20 one time and the movement of the carbon rubbing on itself turned everything in the tank black.  My poor sponges still have a black layer inside causing them to look gray and that was over a year ago, probably 2.
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Post Options Post Options   Thanks (0) Thanks(0)   Quote fj40fax Quote  Post ReplyReply Direct Link To This Post Posted: October 05 2006 at 2:23pm
Looks great Jon!  Do they sell scrap acrylic tubing by the pound at Regional Supply?  I am definately going to make one of these.  I just remembered that I have an old skimmer (air stone) that would be perfect for this.  It may even have another tube inside a tube so I can make both reactors.  Great Idea!!!

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Edited by fj40fax - October 05 2006 at 2:24pm
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Post Options Post Options   Thanks (0) Thanks(0)   Quote jfinch Quote  Post ReplyReply Direct Link To This Post Posted: October 05 2006 at 3:31pm
 Do they sell scrap acrylic tubing by the pound at Regional Supply? 
 
No, the don't sell scrap tubing, but the do sell it by the foot.  And it's relatively cheap (~$2-3/ft for 3" tube).
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Post Options Post Options   Thanks (0) Thanks(0)   Quote Bob Kripfgans Quote  Post ReplyReply Direct Link To This Post Posted: October 05 2006 at 6:54pm
Nice job as usual Jon. Sounds like a good project for a rainy winter weekend.
 
I'm thinking that I could eally use one since I use tap water for top offs. I haven't had to much of a problem with cyno but it could sneak up on me fast.
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Post Options Post Options   Thanks (0) Thanks(0)   Quote Corey Price Quote  Post ReplyReply Direct Link To This Post Posted: October 09 2006 at 11:58pm
I hope to get my DIY skills up to this point. 
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Post Options Post Options   Thanks (0) Thanks(0)   Quote Kevin Quote  Post ReplyReply Direct Link To This Post Posted: October 10 2006 at 10:20am
What is the wall thickness on that acrylic tube?
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Post Options Post Options   Thanks (0) Thanks(0)   Quote Corey Price Quote  Post ReplyReply Direct Link To This Post Posted: October 10 2006 at 1:41pm
I just bought some 1/2" and 3/8" sheet acrylic scraps at Regional- they sell it by the pound.  3" dia extruded tube is less than $4 a foot at Regional, and 4" dia is about $7.50 per foot. 

Edited by Corwando - October 10 2006 at 5:59pm
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Post Options Post Options   Thanks (0) Thanks(0)   Quote jfinch Quote  Post ReplyReply Direct Link To This Post Posted: October 10 2006 at 3:17pm
Almost everything I've built that needed tube was 1/8", but for this particular project I used a piece of 1/4" thick tube that I had laying around.
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Post Options Post Options   Thanks (0) Thanks(0)   Quote Kevin Quote  Post ReplyReply Direct Link To This Post Posted: October 10 2006 at 5:01pm
NEVER MIND -- I just went up and read his post again and found the info I needed.


I previously asked --
Another question, where do you get the rubber gasket for between the acrylic tube plate, and the acrylic plate with all the hose connections?

Edited by Kevin - October 10 2006 at 5:02pm
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